1WCB
PLP-DEPENDENT CATALYTIC ANTIBODY 15A9 IN COMPLEX WITH ITS HAPTEN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-02-24 |
Detector | ADSC CCD |
Spacegroup name | P 1 |
Unit cell lengths | 57.900, 60.300, 64.600 |
Unit cell angles | 79.40, 78.20, 80.80 |
Refinement procedure
Resolution | 40.000 - 2.500 |
R-factor | 0.223 |
Rwork | 0.223 |
R-free | 0.28990 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1clo |
RMSD bond length | 0.075 |
RMSD bond angle | 1.436 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.540 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.080 | 0.200 |
Number of reflections | 28522 | |
<I/σ(I)> | 15.9 | 5.1 |
Completeness [%] | 98.5 | 94.3 |
Redundancy | 1.9 | 1.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 289 | 30% PEG 3350, 200MM SODIUM REMARK 280 IODIDE, 50MM SODIUM ACETATE, PH 6, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 289K |