1W9S
Structure of a beta-1,3-glucan binding CBM6 from Bacillus halodurans
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 113 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV |
Spacegroup name | P 1 |
Unit cell lengths | 30.795, 40.834, 56.118 |
Unit cell angles | 108.95, 105.93, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.590 |
R-factor | 0.119 |
Rwork | 0.117 |
R-free | 0.16600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1gmm |
RMSD bond length | 0.018 |
RMSD bond angle | 1.615 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0003) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.650 |
High resolution limit [Å] | 1.590 | 1.590 |
Rmerge | 0.030 | 0.170 |
Number of reflections | 28471 | |
<I/σ(I)> | 24.9 | 5.7 |
Completeness [%] | 90.1 | 68.5 |
Redundancy | 3.7 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |