1W8D

Binary structure of human DECR.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID29
Synchrotron site	ESRF
Beamline	ID29
Temperature [K]	100
Detector technology	CCD
Collection date	2003-11-07
Detector	ADSC CCD
Spacegroup name	P 1 21 1
Unit cell lengths	62.873, 131.702, 70.592
Unit cell angles	90.00, 92.56, 90.00

Refinement procedure

Resolution	70.710 - 2.200
R-factor	0.221
Rwork	0.219
R-free	0.26500
Structure solution method	OTHER
RMSD bond length	0.010
RMSD bond angle	1.238
Data reduction software	MOSFLM
Data scaling software	SCALA
Refinement software	REFMAC (5.1.24)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	2.320	2.320
High resolution limit [Å]	2.200	2.200
Rmerge	0.080	0.510
Number of reflections	56224
<I/σ(I)>	11.9	1.7
Completeness [%]	96.9	96.9
Redundancy	3.8	3.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7.4		pH 7.40