1W7C
PPLO at 1.23 Angstroms
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-04-01 |
Detector | ADSC CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 139.948, 67.027, 108.688 |
Unit cell angles | 90.00, 118.95, 90.00 |
Refinement procedure
Resolution | 24.010 - 1.230 |
R-factor | 0.113 |
Rwork | 0.112 |
R-free | 0.14600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1n9e |
RMSD bond length | 0.012 |
RMSD bond angle | 1.473 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.000 | 1.270 |
High resolution limit [Å] | 1.240 | 1.230 |
Rmerge | 0.040 | 0.512 |
Number of reflections | 272737 | |
<I/σ(I)> | 12.77 | 2.1 |
Completeness [%] | 95.4 | 94.8 |
Redundancy | 2.78 | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 300 | 35% MPD, IMIDAZOLE PH 8.0, 200 MILLIMOLAR MGCL2, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 300K. |