1W5I
ABA does not affect topology of pLI.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 93 |
| Collection date | 2004-07-05 |
| Spacegroup name | P 41 3 2 |
| Unit cell lengths | 79.222, 79.222, 79.222 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 55.900 - 2.300 |
| R-factor | 0.234 |
| Rwork | 0.231 |
| R-free | 0.29500 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.048 |
| RMSD bond angle | 3.313 |
| Data reduction software | CrystalClear ((MSC/RIGAKU)) |
| Data scaling software | CrystalClear ((MSC/RIGAKU)) |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 35.430 |
| High resolution limit [Å] | 2.300 |
| Rmerge | 0.070 |
| Number of reflections | 3912 |
| <I/σ(I)> | 14 |
| Completeness [%] | 99.8 |
| Redundancy | 5.14 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | HANGING DROP, 1 UL OF 10MG/ML PEPTIDE IN WATER TO 1UL OF 2M NACL 10% PEG 6K. |
