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1W52

Crystal structure of a proteolyzed form of pancreatic lipase related protein 2 from horse

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID14-2
Synchrotron siteESRF
BeamlineID14-2
Temperature [K]100
Detector technologyCCD
Collection date2004-04-04
DetectorADSC CCD
Spacegroup nameP 32 2 1
Unit cell lengths128.426, 128.426, 85.818
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution26.170 - 2.990
R-factor0.234
Rwork0.231
R-free0.29400
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1bu8
RMSD bond length0.020
RMSD bond angle1.993
Data reduction softwareMOSFLM
Data scaling softwareSCALE
Phasing softwareMOLREP
Refinement softwareREFMAC (5.1.24)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]46.0003.150
High resolution limit [Å]2.9902.990
Rmerge0.1300.470
Number of reflections16857
<I/σ(I)>5.41.6
Completeness [%]100.0100
Redundancy13.612.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
18.5pH 8.50

226707

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