1W4T
X-ray crystallographic structure of Pseudomonas aeruginosa arylamine N-acetyltransferase
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 81.667, 81.667, 79.580 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 70.710 - 1.950 |
| R-factor | 0.19 |
| Rwork | 0.188 |
| R-free | 0.21800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.690 |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 36.510 | 2.110 |
| High resolution limit [Å] | 1.340 | 2.000 |
| Rmerge | 0.090 | 0.270 |
| Number of reflections | 21298 | |
| <I/σ(I)> | 5.29 | 2.51 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 7.58 | 5.47 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
