1W41
T. celer L30e E90A variant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX14.1 |
Synchrotron site | SRS |
Beamline | PX14.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 23.023, 53.889, 34.047 |
Unit cell angles | 90.00, 109.22, 90.00 |
Refinement procedure
Resolution | 32.110 - 1.700 |
R-factor | 0.175 |
Rwork | 0.174 |
R-free | 0.19800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1h7m |
RMSD bond length | 0.013 |
RMSD bond angle | 1.399 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0003) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 21.700 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.070 | 0.080 |
Number of reflections | 8679 | |
<I/σ(I)> | 19.1 | 13.4 |
Completeness [%] | 99.6 | 99.8 |
Redundancy | 4 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | pH 6.50 |