1W3Q
NimA from D. radiodurans with covalenly bound lactate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 99.803, 38.773, 60.001 |
Unit cell angles | 90.00, 114.05, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.880 |
R-factor | 0.172 |
Rwork | 0.169 |
R-free | 0.22400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1w3o |
RMSD bond length | 0.014 |
RMSD bond angle | 1.514 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | REFMAC (5.2.0003) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | |
High resolution limit [Å] | 1.880 | |
Rmerge | 0.080 | 0.470 |
Number of reflections | 17262 | |
<I/σ(I)> | 9.9 | 2.2 |
Completeness [%] | 99.8 | 100 |
Redundancy | 2.5 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |