1W1R
Plant Cytokinin Dehydrogenase in Complex with trans-Zeatin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ELETTRA BEAMLINE 5.2R |
Synchrotron site | ELETTRA |
Beamline | 5.2R |
Temperature [K] | 100 |
Collection date | 2004-10-01 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 171.033, 171.033, 54.143 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.000 - 1.900 |
R-factor | 0.206 |
Rwork | 0.205 |
R-free | 0.22400 |
Structure solution method | OTHER |
RMSD bond length | 0.006 |
RMSD bond angle | 1.152 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | CCP4 |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.110 | 0.460 |
Number of reflections | 63311 | |
<I/σ(I)> | 11.2 | 2.7 |
Completeness [%] | 98.9 | 97.9 |
Redundancy | 4.4 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.6 | pH 4.60 |