1W1Q
Plant Cytokinin Dehydrogenase in Complex with Isopentenyladenine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Collection date | 2003-10-04 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 171.356, 171.356, 54.175 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.000 - 1.800 |
R-factor | 0.206 |
Rwork | 0.205 |
R-free | 0.22100 |
Structure solution method | OTHER |
RMSD bond length | 0.007 |
RMSD bond angle | 1.126 |
Phasing software | CCP4 |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.100 | 0.400 |
Number of reflections | 64030 | |
<I/σ(I)> | 13.4 | 2.9 |
Completeness [%] | 99.6 | 99.1 |
Redundancy | 4.5 | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.6 | pH 4.60 |