1W12

UROKINASE TYPE PLASMINOGEN ACTIVATOR

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	295
Spacegroup name	P 41 21 2
Unit cell lengths	55.006, 55.006, 151.609
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	200.000 - 2.400
R-factor	0.1994
Rwork	0.199
R-free	0.26100
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	1.425
Refinement software	CNS

Data quality characteristics

	Overall
Low resolution limit [Å]	200.000
High resolution limit [Å]	2.400
Rmerge	0.140
Number of reflections	9763
Completeness [%]	99.9
Redundancy	5.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1