1W0Z

Urokinase type plasminogen activator

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	296
Spacegroup name	P 21 21 21
Unit cell lengths	53.210, 54.670, 82.400
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	200.000 - 1.900
R-factor	0.199
Rwork	0.199
R-free	0.22080
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	1.264
Refinement software	CNS

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	500.000
High resolution limit [Å]	1.900	1.900
Rmerge	0.088
Number of reflections	18013
Completeness [%]	98.0
Redundancy	3.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		277