1W0X
Crystal structure of human CDK2 in complex with the inhibitor olomoucine.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 287 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU IMAGE PLATE |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 73.770, 72.550, 54.060 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.200 |
R-factor | 0.19 |
Rwork | 0.190 |
R-free | 0.27000 |
Structure solution method | OTHER |
RMSD bond length | 0.013 |
RMSD bond angle | 1.700 |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.200 |
Rmerge | 0.080 |
Number of reflections | 15044 |
Completeness [%] | 99.0 |
Redundancy | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |