1W0O

Vibrio cholerae sialidase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-2
Synchrotron site	ESRF
Beamline	ID14-2
Temperature [K]	100
Spacegroup name	P 21 21 21
Unit cell lengths	70.310, 74.910, 151.615
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	100.000 - 1.900
R-factor	0.1794
Rwork	0.179
R-free	0.21780
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	1.316
Refinement software	CNS (1.0)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.900
Rmerge	0.100
Number of reflections	63699
Completeness [%]	91.0
Redundancy	6.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1