1VYM
NATIVE HUMAN PCNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX9.6 |
Synchrotron site | SRS |
Beamline | PX9.6 |
Temperature [K] | 100 |
Collection date | 2000-02-15 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 136.650, 83.265, 71.634 |
Unit cell angles | 90.00, 117.49, 90.00 |
Refinement procedure
Resolution | 14.000 - 2.300 |
R-factor | 0.191 |
Rwork | 0.187 |
R-free | 0.27900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1axc |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.000 | 2.340 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.058 | 0.450 |
Number of reflections | 31758 | |
<I/σ(I)> | 18.4 | 2.6 |
Completeness [%] | 99.4 | 98.5 |
Redundancy | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 20% PEG3350, 0.2M MAGNESIUM ACETATE, pH 7.00 |