1VXD
NATIVE SPERM WHALE MYOGLOBIN
Experimental procedure
| Temperature [K] | 277 |
| Detector technology | IMAGE PLATE |
| Collection date | 1992-12-31 |
| Detector | RIGAKU RAXIS IIC |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 64.559, 30.865, 34.795 |
| Unit cell angles | 90.00, 106.06, 90.00 |
Refinement procedure
| Resolution | 5.000 - 1.700 |
| R-factor | 0.153 |
| Rwork | 0.153 |
| RMSD bond length | 0.018 |
| RMSD bond angle | 1.945 |
| Data reduction software | RIGAKU |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 1.700 |
| Rmerge | 0.047 |
| Number of reflections | 14498 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Batch method * | 5 | pH 5.0 |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | ammonium salfate | 75 (%sat) |
