1VTB
THE HEXAGONAL CRYSTAL STRUCTURE OF THE A-DNA OCTAMER D(GTGTACAC) AND ITS COMPARISON WITH THE TETRAGONAL STRUCTURE CORRELATED VARIATIONS IN HELICAL PARAMETERS
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Detector technology | OSCILLATION CAMERA |
| Detector | ARNDT-WONACOTT |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 32.400, 32.400, 79.250 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | ? - 2.000 |
| R-factor | 0.127 |
| Refinement software | NUCLSQ |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.000 |
| Number of reflections | 1683 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 278 | VAPOR DIFFUSION, temperature 278.00K |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | 2 | 3 |
| 2 | 1 | 1 | MPD | 5 | 6 |
| 3 | 1 | 1 | MGCL2 | 8 | 9 |
| 4 | 1 | 1 | SPERMINE | 11 | 12 |
| 5 | 1 | 2 | WATER | 14 | 15 |
| 6 | 1 | 2 | MPD | 17 | 18 |
