Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU300 |
| Temperature [K] | 295 |
| Detector technology | IMAGE PLATE |
| Collection date | 1998-11-01 |
| Detector | RIGAKU RAXIS IV |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 96.690, 96.690, 258.600 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 8.000 - 2.400 |
| R-factor | 0.193 |
| Rwork | 0.193 |
| R-free | 0.25400 |
| Structure solution method | AB INITIO |
| RMSD bond length | 0.000 |
| RMSD bond angle | 0.020 |
| Data scaling software | SCALEPACK |
| Phasing software | SHELX |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 8.000 | 2.490 |
| High resolution limit [Å] | 2.400 | 2.400 |
| Rmerge | 0.107 | 0.740 |
| Number of reflections | 53535 | |
| <I/σ(I)> | 10.1 | |
| Completeness [%] | 89.5 | 78 |
| Redundancy | 1.99 | 1.64 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4 | 296 | 2.2M NaCl 0.1M Sodium Citrate (pH4) 0.3M manoheptose, VAPOR DIFFUSION, HANGING DROP, temperature 296K |
