1VPT
AS11 VARIANT OF VACCINIA VIRUS PROTEIN VP39 IN COMPLEX WITH S-ADENOSYL-L-METHIONINE
Experimental procedure
Temperature [K] | 103 |
Detector technology | IMAGE PLATE |
Collection date | 1995-12-13 |
Detector | MAC Science DIP-2030 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 85.300, 67.800, 80.400 |
Unit cell angles | 90.00, 118.40, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.800 |
R-factor | 0.215 |
Rwork | 0.215 |
R-free | 0.25000 |
Structure solution method | MIRAS |
RMSD bond length | 0.010 |
RMSD bond angle | 1.770 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASES |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 1.920 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.050 | 0.250 |
Total number of observations | 208238 * | |
Number of reflections | 33404 | |
<I/σ(I)> | 39.8 | 6.2 |
Completeness [%] | 98.0 | 88.6 |
Redundancy | 3.4 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 4.5 | pH 4.5 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | PEG8000 | 10 (%) | |
2 | 1 | 1 | 0.125 (M) | ||
3 | 1 | 1 | citrate | 0.1 (M) |