1VNS
RECOMBINANT APO-CHLOROPEROXIDASE FROM CURVULARIA INAEQUALIS
Experimental procedure
Source type | SYNCHROTRON |
Source details | MPG/DESY, HAMBURG BEAMLINE BW6 |
Synchrotron site | MPG/DESY, HAMBURG |
Beamline | BW6 |
Temperature [K] | 100 |
Collection date | 1997-12 |
Spacegroup name | H 3 |
Unit cell lengths | 130.040, 130.040, 112.150 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 1.660 |
R-factor | 0.179 * |
Rwork | 0.180 |
R-free | 0.21600 * |
Structure solution method | OTHER |
RMSD bond length | 0.007 |
RMSD bond angle | 1.670 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 1.690 |
High resolution limit [Å] | 1.660 | 1.660 |
Rmerge | 0.069 * | 0.339 * |
Total number of observations | 430434 * | |
Number of reflections | 81916 | |
<I/σ(I)> | 7 | 2.3 |
Completeness [%] | 99.0 | 99 |
Redundancy | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7.5 * | pH 8.0 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 5 (mg/ml) | |
2 | 1 | drop | MOPS | 5 (mM) | |
3 | 1 | drop | vanadate | 1 (mM) | |
4 | 1 | reservoir | ammonium sulfate | 0.85 (M) | |
5 | 1 | reservoir | Tris-H2SO4 | 0.05 (M) | |
6 | 1 | reservoir | sodium vanadate | 0.5 (mg/ml) | |
7 | 1 | reservoir | l-cysteine | 0.05 (M) |