1VNI
CHLOROPEROXIDASE FROM THE FUNGUS CURVULARIA INAEQUALIS: RECOMBINANT HOLO-CHLOROPEROXIDASE
Experimental procedure
Temperature [K] | 287 |
Collection date | 1998-06 |
Spacegroup name | H 3 |
Unit cell lengths | 131.840, 131.840, 112.830 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 2.150 |
R-factor | 0.181 * |
Rwork | 0.180 |
R-free | 0.22600 * |
Structure solution method | OTHER |
RMSD bond length | 0.006 |
RMSD bond angle | 1.570 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 2.270 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.069 * | 0.278 * |
Total number of observations | 164218 * | |
Number of reflections | 39327 | |
<I/σ(I)> | 6.2 | 2.4 |
Completeness [%] | 99.2 | 95.6 |
Redundancy | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7.5 * | 4 * | pH 8.0 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 5 (mg/ml) | |
2 | 1 | drop | MOPS | 5 (mM) | |
3 | 1 | drop | vanadate | 1 (mM) | |
4 | 1 | reservoir | ammonium sulfate | 0.85 (M) | |
5 | 1 | reservoir | Tris-H2SO4 | 0.05 (M) | |
6 | 1 | reservoir | sodium vanadate | 0.5 (mg/ml) | |
7 | 1 | reservoir | l-cysteine | 0.05 (M) |