1VLT

LIGAND BINDING DOMAIN OF THE WILD-TYPE ASPARTATE RECEPTOR WITH ASPARTATE

Experimental procedure

Detector technology	IMAGE PLATE
Detector	RIGAKU
Spacegroup name	P 21 21 21
Unit cell lengths	60.670, 72.740, 73.260
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 2.200
R-factor	0.198
Rwork	0.198
RMSD bond length	0.013 *
RMSD bond angle	1.760 *
Data reduction software	MSC
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	6.000 *
High resolution limit [Å]	2.190 *
Rmerge	0.079
Total number of observations	56261 *
Number of reflections	15964 *
Redundancy	3.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir		0.1 (M)
2	1	reservoir	acetate	0.1 (M)
3	1	reservoir	PEG400	40 (%)
4	1	drop		0.05 (M)
5	1	drop	acetate	0.05 (M)
6	1	drop	PEG400	20 (%)
7	1	drop	aspartate	5 (mM)