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1VKM

Crystal structure of an indigoidine synthase a (idga)-like protein (tm1464) from thermotoga maritima msb8 at 1.90 A resolution

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 8.2.1
Synchrotron siteALS
Beamline8.2.1
Temperature [K]100
Detector technologyCCD
Collection date2003-10-12
DetectorADSC
Spacegroup nameP 21 21 21
格子定数 [Å]91.958, 130.799, 138.750
格子定数 [度]90.00, 90.00, 90.00
精密化法
分解能75.230 - 1.900
R因子0.15618
Rwork0.154
R-free0.19959
Structure solution methodMAD
結合長の平均二乗偏差(RMSD) [Å]0.017
結合角の平均二乗偏差(RMSD) [度]1.514
Data reduction softwareMOSFLM
Data scaling softwareSCALA (4.2))
Phasing softwareSOLVE
Refinement softwareREFMAC (5.2.0000)
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)75.2301.950
分解能 [Å] (高)1.9001.900
Rmerge_l_obs0.0630.533
独立反射数130700
<I/σ(I)>13.71.9
完全性 [%]99.193.3
冗長性4.72.8
結晶化条件
結晶ID方法pH温度溶液条件
1VAPOR DIFFUSION,SITTING DROP,NANODROP7.42777% PEG 1000, 0.045M HEPES_Na, 0.055M HEPES, 0.01M MANGANESE (II) CHLORIDE, pH 7.4, VAPOR DIFFUSION,SITTING DROP,NANODROP, temperature 277K
1VAPOR DIFFUSION,SITTING DROP,NANODROP7.42777% PEG 1000, 0.045M HEPES_Na, 0.055M HEPES, 0.01M MANGANESE (II) CHLORIDE, pH 7.4, VAPOR DIFFUSION,SITTING DROP,NANODROP, temperature 277K
1VAPOR DIFFUSION,SITTING DROP,NANODROP7.42777% PEG 1000, 0.045M HEPES_Na, 0.055M HEPES, 0.01M MANGANESE (II) CHLORIDE, pH 7.4, VAPOR DIFFUSION,SITTING DROP,NANODROP, temperature 277K

239803

件を2025-08-06に公開中

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