1VKL
RABBIT MUSCLE PHOSPHOGLUCOMUTASE
Experimental procedure
Temperature [K] | 289 |
Detector technology | AREA DETECTOR |
Collection date | 1993-10 |
Detector | XUONG-HAMLIN MULTIWIRE |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 174.420, 174.420, 101.120 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.700 |
R-factor | 0.17 |
Rwork | 0.170 |
R-free | 0.21000 |
Starting model (for MR) | 3pmg |
RMSD bond length | 0.013 |
RMSD bond angle | 24.543 * |
Data reduction software | XDS |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.600 |
Rmerge | 0.150 |
Number of reflections | 46280 |
Completeness [%] | 97.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 6.4 | Lin, Z., (1986) J.Biol.Chem., 261, 264. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | ammonium salfate | 47 (%sat) | |
2 | 1 | 1 | PEG400 | 3-4 (%) |