1VIJ

HIV-1 PROTEASE COMPLEXED WITH THE INHIBITOR HOE/BAY 793 HEXAGONAL FORM

Experimental procedure

Spacegroup name	P 61
Unit cell lengths	64.270, 64.270, 82.930
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	8.000 - 2.400
R-factor	0.178
RMSD bond length	0.014
RMSD bond angle	4.400
Refinement software	PROLSQ

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	2.400 *	2.400 *
Rmerge	0.070 *
Total number of observations	18894 *
Number of reflections	5468 *
Completeness [%]	90.0 *	93 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	5.8 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	3 (mg/ml)
2	1	drop	sodium acetate	50 (mM)
3	1	drop	inhibitor	1 (mg/ml)	in Me2SO
4	1	reservoir	ammonium sulfate	30 (%)