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1VGL

Crystal structure of tetrameric KaiB from T.elongatus BP-1

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsSPRING-8 BEAMLINE BL41XU
Synchrotron siteSPring-8
BeamlineBL41XU
Temperature [K]100
Detector technologyCCD
DetectorMARRESEARCH
Wavelength(s)1.0080
Spacegroup nameP 1 2 1
Unit cell lengths63.740, 33.410, 93.740
Unit cell angles90.00, 100.12, 90.00
Refinement procedure
Resolution20.000 - 2.600
R-factor0.23
Rwork0.227
R-free0.28900
Structure solution methodMAD
RMSD bond length0.013
RMSD bond angle1.659
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareSOLVE
Refinement softwareREFMAC (5.0)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]100.0002.740
High resolution limit [Å]2.6002.600
Number of reflections12369
Completeness [%]100.0100
Redundancy3.83.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP4.5293PEG 3350, DMSO, acetate, pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K

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