1VG6
Crystal Structure Of Octaprenyl Pyrophosphate Synthase From Hyperthermophilic Thermotoga Maritima F132A/L128A/I123A mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Detector technology | IMAGE PLATE |
Collection date | 2003-10-22 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 151.969, 151.969, 64.243 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.240 - 3.350 |
Rwork | 0.241 |
R-free | 0.29010 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1v4e |
RMSD bond length | 0.003 |
RMSD bond angle | 0.720 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.470 |
High resolution limit [Å] | 3.350 | 3.350 |
Rmerge | 0.100 | 0.556 |
Number of reflections | 5051 | |
<I/σ(I)> | 15.51 | 3.17 |
Completeness [%] | 89.0 | 87.7 |
Redundancy | 5.65 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | Hepes, Lithium sulfate, PEG 900, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K |