1VDS
The crystal structure of the tetragonal form of hen egg white lysozyme at 1.6 angstroms resolution in space
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Collection date | 1997-05-27 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 79.192, 79.192, 37.933 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 9.880 - 1.600 |
R-factor | 0.185 |
Rwork | 0.185 |
R-free | 0.21900 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 2.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 17.600 | 1.660 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.061 | 0.145 |
Number of reflections | 15634 | |
<I/σ(I)> | 19 | |
Completeness [%] | 94.8 | 98.7 |
Redundancy | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |