1VBO
Crystal structure of artocarpin-mannotriose complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 278 |
Detector technology | IMAGE PLATE |
Collection date | 2003-06-10 |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 138.217, 72.296, 59.373 |
Unit cell angles | 90.00, 94.48, 90.00 |
Refinement procedure
Resolution | 19.850 - 2.350 |
R-factor | 0.209 |
Rwork | 0.209 |
R-free | 0.22600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1j4u |
RMSD bond length | 0.018 |
RMSD bond angle | 3.400 |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.430 |
High resolution limit [Å] | 2.350 | 2.350 |
Rmerge | 0.104 | 0.498 |
Number of reflections | 48504 | |
<I/σ(I)> | 8.9 | |
Completeness [%] | 99.2 | 99.3 |
Redundancy | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 300 | PEG4000, PEG1450, Phosphate buffer, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 300K |