1V8U
Crystal structure analysis of the ADP-ribose pyrophosphatase of E82Q mutant with SO4 and Mg
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS |
Wavelength(s) | 1.54 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 49.860, 49.860, 117.920 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.550 - 1.900 |
R-factor | 0.208 |
Rwork | 0.203 |
R-free | 0.22100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 1.400 |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.550 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 13320 | |
Completeness [%] | 95.1 | 86.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | VAPOR DIFFUSION, HANGING DROP, temperature 293K |