1V8S

Crystal structure analusis of the ADP-ribose pyrophosphatase complexed with AMP and Mg

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU
Detector technology	IMAGE PLATE
Detector	RIGAKU RAXIS
Wavelength(s)	1.54
Spacegroup name	P 32 2 1
Unit cell lengths	49.740, 49.740, 118.120
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	34.800 - 2.200
R-factor	0.199
Rwork	0.199
R-free	0.24800
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	1.300
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	39.370	2.280
High resolution limit [Å]	2.200	2.200
Number of reflections	8302
Completeness [%]	91.1	85.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	VAPOR DIFFUSION, HANGING DROP, temperature 293K