1V8L

Structure Analysis of the ADP-ribose pyrophosphatase complexed with ADP-ribose

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Detector technology	IMAGE PLATE
Detector	RIGAKU RAXIS IV
Wavelength(s)	1.54
Spacegroup name	P 32 2 1
Unit cell lengths	49.771, 49.771, 119.330
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	16.140 - 2.100
R-factor	0.217
Rwork	0.217
R-free	0.24000
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.013
RMSD bond angle	2.000
Phasing software	AMoRE
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	2.120
High resolution limit [Å]	2.010	2.010
Number of reflections	11986
Completeness [%]	99.9	99.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1