1V6Z
Crystal structure of TT1573 from Thermus thermophilus
Experimental procedure
| Experimental method | SAD |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL44B2 |
| Synchrotron site | SPring-8 |
| Beamline | BL44B2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-10-02 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.9790 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 54.406, 78.506, 54.871 |
| Unit cell angles | 90.00, 114.43, 90.00 |
Refinement procedure
| Resolution | 49.960 - 2.000 |
| Rwork | 0.197 |
| R-free | 0.24600 |
| Structure solution method | SAD |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.400 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.960 | 2.070 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Number of reflections | 28450 | |
| <I/σ(I)> | 39 | 15.4 |
| Completeness [%] | 99.9 | 99.4 |
| Redundancy | 9.8 | 5.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 297 | 25% PEG3350, 0.2M Potassium Formate, VAPOR DIFFUSION, HANGING DROP, temperature 297K |
