1V6P
Crystal structure of Cobrotoxin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE F1 |
| Synchrotron site | CHESS |
| Beamline | F1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Wavelength(s) | 0.93 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 46.808, 47.287, 90.018 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 - 0.870 |
| Rwork | 0.119 |
| R-free | 0.15330 |
| Structure solution method | AB INITIO |
| RMSD bond length | 0.015 |
| RMSD bond angle | 0.038 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 0.890 |
| High resolution limit [Å] | 0.870 | 0.870 |
| Rmerge | 0.062 | 0.426 |
| Number of reflections | 76069 | |
| Completeness [%] | 92.8 | 38.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 293 | HAc-NaAc, Ethanol, NaCl, CuCl2, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
