1V2X
TrmH
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL41XU |
| Synchrotron site | SPring-8 |
| Beamline | BL41XU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2002-06-26 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.9 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 77.601, 44.023, 56.756 |
| Unit cell angles | 90.00, 120.78, 90.00 |
Refinement procedure
| Resolution | 34.370 - 1.500 |
| R-factor | 0.225 |
| Rwork | 0.225 |
| R-free | 0.27700 |
| Structure solution method | MAD |
| RMSD bond length | 0.014 |
| RMSD bond angle | 2.000 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | SHARP |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.000 | |
| High resolution limit [Å] | 1.500 | 1.500 |
| Number of reflections | 60955 | |
| <I/σ(I)> | 9.5 | 1.6 |
| Completeness [%] | 91.8 | 81.5 |
| Redundancy | 2.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | lithium sulfate, Tris-HCl, PEG 4000, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
