1V2T
Trypsin inhibitor in complex with bovine trypsin variant X(SSFI.Glu)bT.B4
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU300 |
| Temperature [K] | 287 |
| Detector technology | IMAGE PLATE |
| Collection date | 2002-07-25 |
| Detector | RIGAKU RAXIS IV |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 55.130, 58.240, 67.810 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 - 1.900 |
| Rwork | 0.211 |
| R-free | 0.23700 |
| Structure solution method | FOURIER SYNTHESIS |
| Data reduction software | CrystalClear |
| Data scaling software | CrystalClear |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 44.180 |
| High resolution limit [Å] | 1.440 |
| Number of reflections | 33170 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 294 | ammonium sulphate, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 294K |
