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1V2P

Trypsin inhibitor in complex with bovine trypsin variant X(SSYI)bT.A4

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU300
Temperature [K]287
Detector technologyIMAGE PLATE
Collection date2002-06-23
DetectorRIGAKU RAXIS IV
Spacegroup nameP 31 2 1
Unit cell lengths55.080, 55.080, 109.750
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution10.000 - 1.920
Rwork0.213
R-free0.25500
Structure solution methodFOURIER SYNTHESIS
Data reduction softwareCrystalClear
Data scaling softwareCrystalClear
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 Overall
Low resolution limit [Å]43.750
High resolution limit [Å]1.440
Number of reflections29106
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP8293ammonium sulphate, pH 8, VAPOR DIFFUSION, HANGING DROP, temperature 293K

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