1V2O
Trypsin inhibitor in complex with bovine trypsin variant X(SSYI)bT.B4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 287 |
Detector technology | IMAGE PLATE |
Collection date | 2002-08-27 |
Detector | RIGAKU RAXIS IV |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 55.110, 58.020, 68.520 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.620 |
Rwork | 0.183 |
R-free | 0.19600 |
Structure solution method | FOURIER SYNTHESIS |
Data reduction software | CrystalClear |
Data scaling software | CrystalClear |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 100.000 |
High resolution limit [Å] | 1.620 |
Number of reflections | 28576 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | ammonium sulphate, pH 8, VAPOR DIFFUSION, HANGING DROP, temperature 293K |