1V2L
Benzamidine in complex with bovine trypsin variant X(triple.Glu)bT.D1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 287 |
Detector technology | IMAGE PLATE |
Collection date | 2002-08-17 |
Detector | RIGAKU RAXIS IV |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 54.680, 54.680, 136.460 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 1.600 |
Rwork | 0.189 |
R-free | 0.19900 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | CrystalClear |
Data scaling software | CrystalClear |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 47.350 |
High resolution limit [Å] | 1.500 |
Number of reflections | 36155 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 313 | ammonium sulphate, pH 6, VAPOR DIFFUSION, HANGING DROP, temperature 313K |