1V1P
The structure SSL from Staphylococcus Aureus from an orthorhombic crystal form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-08-15 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 51.653, 71.598, 103.471 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 58.722 - 2.700 |
R-factor | 0.23526 |
Rwork | 0.232 |
R-free | 0.30070 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1m4v |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 31.010 | 2.850 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.140 | 0.490 |
Number of reflections | 11074 | |
<I/σ(I)> | 4.5902 | 1.53 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 4.5 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 0.1M TRICINE BUFFER @PH 8.5, 28% (W/V) PEG2K, 0.1M LITHIUM SULPHATE |