1V0O
Structure of P. falciparum PfPK5-Indirubin-5-sulphonate ligand complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-1 |
| Synchrotron site | ESRF |
| Beamline | ID14-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 60.562, 88.277, 63.857 |
| Unit cell angles | 90.00, 97.33, 90.00 |
Refinement procedure
| Resolution | 63.250 - 1.900 |
| Rwork | 0.233 |
| R-free | 0.28178 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 25.080 |
| High resolution limit [Å] | 1.900 |
| Rmerge | 0.015 |
| Number of reflections | 49359 |
| Completeness [%] | 94.1 |
| Redundancy | 2.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.4 | pH 7.40 |
