1V00
Erythrina cristagalli lectin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX14.1 |
| Synchrotron site | SRS |
| Beamline | PX14.1 |
| Temperature [K] | 293 |
| Detector technology | CCD |
| Collection date | 2002-02-15 |
| Detector | ADSC CCD |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 54.900, 167.230, 55.130 |
| Unit cell angles | 90.00, 97.08, 90.00 |
Refinement procedure
| Resolution | 21.120 - 1.700 |
| R-factor | 0.172 |
| Rwork | 0.172 |
| R-free | 0.19500 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.490 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | CNS (1.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.760 |
| High resolution limit [Å] | 1.700 | 1.700 |
| Rmerge | 0.058 | 0.134 |
| Number of reflections | 108695 | |
| <I/σ(I)> | 28.09 | 5.28 |
| Completeness [%] | 99.9 | 77.3 |
| Redundancy | 1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | 20% PEG 3350, 0.2M IMIDAZOLE, pH 7.00 |
