1UZG
CRYSTAL STRUCTURE OF THE DENGUE TYPE 3 VIRUS ENVELOPE PROTEIN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F1 |
Synchrotron site | CHESS |
Beamline | F1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-10-15 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 52.855, 68.631, 270.180 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.990 - 3.500 |
R-factor | 0.286 |
Rwork | 0.284 |
R-free | 0.32400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1oan |
RMSD bond length | 0.009 |
RMSD bond angle | 1.527 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 21.000 | 3.730 |
High resolution limit [Å] | 3.600 | 3.600 |
Rmerge | 0.120 | 0.538 |
Number of reflections | 12090 | |
<I/σ(I)> | 12.3 | 2.6 |
Completeness [%] | 91.8 | 81.1 |
Redundancy | 5 | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 15% PEG 8K, 0.2 M LICL2, 0.1 M TRIS/HCL, PH 8.5 |