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1UXN

Structural basis for allosteric regulation and substrate specificity of the non-phosphorylating glyceraldehyde-3-phosphate dehydrogenase (GAPN) from Thermoproteus tenax

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsEMBL/DESY, HAMBURG BEAMLINE BW7B
Synchrotron siteEMBL/DESY, HAMBURG
BeamlineBW7B
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2001-08-15
DetectorMAR scanner 345 mm plate
Spacegroup nameP 62 2 2
Unit cell lengths185.520, 185.520, 134.120
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution30.000 - 2.300
R-factor0.206
Rwork0.206
R-free0.23300
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1ky8
RMSD bond length0.011
RMSD bond angle1.700
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Refinement softwareCNS (1.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.400
High resolution limit [Å]2.3002.300
Rmerge0.0460.380
Number of reflections54271
<I/σ(I)>314
Completeness [%]90.091
Redundancy15.315
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
15.62M SODIUM FORMATE PH 5.6, 0.1 M SODIUM ACETATE PH 5.6, 50 MM AMP

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