1UX0
Bacillus subtilis cytidine deaminase with an Arg56 - Gln substitution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I711 |
Synchrotron site | MAX II |
Beamline | I711 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2001-11-22 |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 74.880, 66.098, 55.514 |
Unit cell angles | 90.00, 115.64, 90.00 |
Refinement procedure
Resolution | 19.950 - 1.990 |
R-factor | 0.191 |
Rwork | 0.191 |
R-free | 0.20700 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 1jtk |
RMSD bond length | 0.004 |
RMSD bond angle | 1.100 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.040 |
High resolution limit [Å] | 1.990 | 1.990 |
Rmerge | 0.106 | 0.351 |
Number of reflections | 16761 | |
<I/σ(I)> | 16.9 | 3.2 |
Completeness [%] | 100.0 | 99.4 |
Redundancy | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 4.6 | VAPOUR DIFFUSION AT RT: PROTEIN: 4.6 MG/ML + 5 MM TETRAHYDRODEOXYURIDINE PRECIPITANT: 17-23 % MPD, 10 MM CALCIUM CHLORIDE 0.1 M SODIUM ACETATE, pH 4.60 |