1UVU
BOVINE THROMBIN--BM12.1700 COMPLEX
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU |
Detector technology | AREA DETECTOR |
Detector | SIEMENS |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 87.040, 87.040, 103.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.800 |
R-factor | 0.226 |
Rwork | 0.226 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 23.700 * |
Data reduction software | SAINT |
Data scaling software | SAINT |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.800 * |
Rmerge | 0.060 |
Number of reflections | 14074 |
Redundancy | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 7 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium sulfate | 1.8 (M) | |
2 | 1 | reservoir | Tris | 0.1 (M) | |
3 | 1 | drop | ammonium sulfate | 0.9 (M) | |
4 | 1 | drop | Tris | 0.05 (M) | |
5 | 1 | drop | protain | 5 (mg/ml) |