1URY

cytoglobin cavities

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF
Synchrotron site	ESRF
Temperature [K]	100
Collection date	2003-08-15
Spacegroup name	P 21 21 21
Unit cell lengths	47.848, 70.524, 98.728
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	29.880 - 2.400
R-factor	0.19983
Rwork	0.197
R-free	0.25442
Structure solution method	OTHER
Data reduction software	MOSFLM
Data scaling software	SCALA
Refinement software	REFMAC

Data quality characteristics

	Overall
Low resolution limit [Å]	30.000
High resolution limit [Å]	2.400
Rmerge	0.100
Number of reflections	13612
Completeness [%]	98.3
Redundancy	3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		5		pH 5.00