1UO1
Structure Based Engineering of Internal Molecular Surfaces Of Four Helix Bundles
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 114 |
Collection date | 2002-10-15 |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 79.391, 79.391, 79.391 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.900 - 2.500 |
R-factor | 0.2347 |
Rwork | 0.231 |
R-free | 0.30246 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | CrystalClear ((MSC/RIGAKU)) |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 35.578 |
High resolution limit [Å] | 2.218 |
Rmerge | 0.094 |
Number of reflections | 3283 |
<I/σ(I)> | 7.5 |
Completeness [%] | 100.0 |
Redundancy | 12.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 2.5 M NACL, 100 MM NAAC, 200 MM LI2SO4, PH 4.5 |