1UMO

The crystal structure of cytoglobin: the fourth globin type discovered in man

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ELETTRA BEAMLINE 5.2R
Synchrotron site	ELETTRA
Beamline	5.2R
Temperature [K]	100
Detector technology	CCD
Collection date	2002-11-15
Detector	MARRESEARCH
Spacegroup name	P 21 21 21
Unit cell lengths	46.617, 72.001, 98.334
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	29.880 - 2.590
R-factor	0.21161
Rwork	0.208
R-free	0.28376
Structure solution method	SAD
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	SOLVE
Refinement software	REFMAC

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	2.690
High resolution limit [Å]	2.600	2.600
Rmerge	0.057	0.159
Number of reflections	19995
<I/σ(I)>	35	11
Completeness [%]	99.5	96.6
Redundancy	11	10

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		4		pH 4.00